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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Deacon, G.B." name="eprints.creators_name" />
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<meta content="Organomercury Compounds XV. The Acceptor Properties of
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<meta content="Crystalline adducts, Ph2Hg.2L (L = l,lO-phenanthroline, 2,9-dimethyl-1,10-phenanthroline, and 2,4,7,9-tetramethyl-l,l0-phenanthroline), have been prepared by reaction of diphenylmercury and the appropriate ligands in hexane, but derivatives of the mercurial with a range of ligands having nitrogen, phosphorus, arsenic and oxygen donor atoms could not be prepared. No definite evidence for coordination cf the phenanthroline ligands in the solid adducts could be obtained by infrared or ultraviolet
spectroscopy. Molecular weights of the adducts in benzene or chloroform showed them to be completely dissociated in solution. Similar measurements for mixtures of the mercurial and a range of ligands in benzene showed no evidence for complex formation. Thus, any acceptor properties of diphenylmercury appear to be very weak." name="eprints.abstract" />
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<meta content="1 (a) R. J. Bertino, G. B. Deacon and F. 3. Taylor, Ausr. J. Chem, in press;
(b)G. B. Deacon and A. 3. Canty, Inorg. Nucl. Chem. Lett., 5 (1969) 183.
2 G. E. Coates. M. L. I-I. Green and K. Wade, Organometallic Compounds, Vol I, Methuen. London. 1967,
pp. 164,158; H. J. Emeleus and J. J. Lagowskii J. Chem. Sot., (1959) 1497; A. J. Downs, J. Znorg. Nud
Chem, 26 (1964) 41.
3 R. D. Chambers, G. E. Coates, J. G. Livingstone and W. K. R. Musgrave. J. Chem Sot_, (1967) 4367_
4 J. E. Connett, A. G. Davies, G. B. Deacbn and 3. H. S. Green. J. Chem. Sot. C, (1966) 106; G. B. Deacon
and P. W. Felder, Aust. J. Chem., 19 (1966) 2381.
5 J. E. Connett and G. B. Deacon, J. Chem. Sot., C, (1966) 1058.
6 H. B. Powell and J. J. Lagowski. J. Chem. Sot. A, (1966) 1282.
7 A. J. Canty and G. B. Deacon, Aust. J. Chem., 21 (1968) 1757.
8 R. D. Chambers. F. G. Drakesmith, J. Hutchinson and W. K. R. Musgrave, Tetrahedron Lett., (1967)
1705; V. I- Bregadze and 0. Yu Okhlobystin, Dokl. Akud. Nnuk SSSR, 177 (1967) 347; L. I. Zakharkin
and L. S. Podvisotskaya, J. Gen. Chem. USSR, 39 (1969) 896; Iza Akad- Nauk SSSR, Ser. Khim.. (1968)
681.
9 A. L. Fridman, T. N. Ivshina, A. Tartakovskii and S. S. Kovikov, Izv. Akad. Nauk SSSR, Ser. Khim..
(1968) 2839; (1969) 2304; G. I. Oleneva T. N. Ivshina and V. A. Shlyapochnikov, Irv. Akad. Nnuk SSSR,
Ser. Khim., (1969) 2822.
10 A. J. Canty and G. B. Deacon, Au.% J. Chem., 24 (1971) 489.
11 W. J. Lile and R. C. Menzies, J. Chem. Sot., (1950) 617.
12 H. B. Powell, M. T. Maung and J. J. Lagowski, J. Chem. Sot., (1963) 2484.
13 L. A. Fedorov and E. I. Fedin, DokL Akud. Nauk SSSR, 195 (1970) 879.
14 J. H. S. Green, Spectrochim. Acca, Part A, 24 (1968) 863.
15 R J. H. Clark and C. S. Williams, Znorg. Chem. 4 (1965) 350; C. W. Frank and L. B. Rogers, Znorg. Chem.,
5 (1966) 615.
18 W.‘R I&Whinnie and ? D. MilIer, A+zn. Inorg. Chk~kadiochek, 12 (1969) 135.
17;E_-C. M. Grigg, J. R. Hall andR &. Plowma?, Aust. J. Chem, 15 (1962) 425.
18 I_ R Beattie and U Webster, J_.Phys. CJim1.,.66 (1962) 115.
19 G. Bahr and G. Meier, 2. &org..AZlg Chem, 294 (1958) 22. .. r
20. A. J. Canty and B. M. Gatehouse, Acfa Crystallogr., S&t. B, 28 (1972) 1872.
21 D_ Grdenic &d f Krstanovik, Arh. Kim., 27 (1955) 143.
22. D. Grdenic, Quart- Rev., Chem SOC., 19 (1965) 303.
23 G. B. Deacon and J. C. Parrott, Ausr. J. Chem, 24 (1971) 1771." name="eprints.referencetext" />
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<meta content="Crystalline adducts, Ph2Hg.2L (L = l,lO-phenanthroline, 2,9-dimethyl-1,10-phenanthroline, and 2,4,7,9-tetramethyl-l,l0-phenanthroline), have been prepared by reaction of diphenylmercury and the appropriate ligands in hexane, but derivatives of the mercurial with a range of ligands having nitrogen, phosphorus, arsenic and oxygen donor atoms could not be prepared. No definite evidence for coordination cf the phenanthroline ligands in the solid adducts could be obtained by infrared or ultraviolet
spectroscopy. Molecular weights of the adducts in benzene or chloroform showed them to be completely dissociated in solution. Similar measurements for mixtures of the mercurial and a range of ligands in benzene showed no evidence for complex formation. Thus, any acceptor properties of diphenylmercury appear to be very weak." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Organomercury Compounds XV. The Acceptor Properties of Diphenylmercury</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Deacon, G.B.</span> (1973) <xhtml:em>Organomercury Compounds XV. The Acceptor Properties of Diphenylmercury.</xhtml:em> Journal of Organometallic Chemistry, 49 (1). pp. 125-132. ISSN 0022-328X</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2871/1/JOMC1973_2C_125.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2871/1/JOMC1973_2C_125.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />1575Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="4098" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1016/S0022-328X(00)84947-5">http://dx.doi.org/10.1016/S0022-328X(00)84947-5</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">Crystalline adducts, Ph2Hg.2L (L = l,lO-phenanthroline, 2,9-dimethyl-1,10-phenanthroline, and 2,4,7,9-tetramethyl-l,l0-phenanthroline), have been prepared by reaction of diphenylmercury and the appropriate ligands in hexane, but derivatives of the mercurial with a range of ligands having nitrogen, phosphorus, arsenic and oxygen donor atoms could not be prepared. No definite evidence for coordination cf the phenanthroline ligands in the solid adducts could be obtained by infrared or ultraviolet
spectroscopy. Molecular weights of the adducts in benzene or chloroform showed them to be completely dissociated in solution. Similar measurements for mixtures of the mercurial and a range of ligands in benzene showed no evidence for complex formation. Thus, any acceptor properties of diphenylmercury appear to be very weak.</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Additional Information:</th><td valign="top" class="ep_row">The definitive version is available at http://www.sciencedirect.com
</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2871</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">15 Jan 2008 15:14</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">15 Jan 2008 15:14</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2871;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2871">item control page</a></p>
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