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<title>UTas ePrints - Synthesis of 1,1-Bis(pyrazol-1 -ylmethyl)ethene and the Structure of a Trimethylplatinum(1V) Derivative containing an Eight-membered Chelate Ring</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Honeyman, R.T." name="eprints.creators_name" />
<meta content="Skelton, B.W." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
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Structure of a Trimethylplatinum(1V) Derivative containing
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<meta content="The bidentate pyrazole-donor ligand 1,1-bis(pyrazo1-1-ylmethyl)ethene, [(pz)CH2]2C=CH2, may be synthesized in high yield on reaction of the readily obtained potassium pyrazolide with commercially available (CICH2)2C=CH2. Reaction of the ligand with [{PtMe2(SEt2)}2], followed by addition of iodomethane, gives the platinum(IV) complex fac-[PtlMe3{[(pz)CH2]2C=CH2-N,N'}]. Proton NMR and X-ray structural studies show that the eight-membered chelate ring PtNNC3NN adopts a configuration in which the pyrazole rings are in different environments, forming angles of 26.0(3) and 38.2(3) with the 'PtC2N2' mean plane. Thus, the four methylene protons are also in different environments, as are the PtMe groups trans to pyrazole groups. The eight-membered chelate ring is fluxional, undergoing inversion with DGact ~ 15 kcal mol-1 (~63 kJ mol-l) at 10 C." name="eprints.abstract" />
<meta content="1992" name="eprints.date" />
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<meta content="The bidentate pyrazole-donor ligand 1,1-bis(pyrazo1-1-ylmethyl)ethene, [(pz)CH2]2C=CH2, may be synthesized in high yield on reaction of the readily obtained potassium pyrazolide with commercially available (CICH2)2C=CH2. Reaction of the ligand with [{PtMe2(SEt2)}2], followed by addition of iodomethane, gives the platinum(IV) complex fac-[PtlMe3{[(pz)CH2]2C=CH2-N,N'}]. Proton NMR and X-ray structural studies show that the eight-membered chelate ring PtNNC3NN adopts a configuration in which the pyrazole rings are in different environments, forming angles of 26.0(3) and 38.2(3) with the 'PtC2N2' mean plane. Thus, the four methylene protons are also in different environments, as are the PtMe groups trans to pyrazole groups. The eight-membered chelate ring is fluxional, undergoing inversion with DGact ~ 15 kcal mol-1 (~63 kJ mol-l) at 10 C." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Synthesis of 1,1-Bis(pyrazol-1 -ylmethyl)ethene and the Structure of a Trimethylplatinum(1V) Derivative containing an Eight-membered Chelate Ring</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Honeyman, R.T.</span> and <span class="person_name">Skelton, B.W.</span> and <span class="person_name">White, A.H.</span> (1992) <xhtml:em>Synthesis of 1,1-Bis(pyrazol-1 -ylmethyl)ethene and the Structure of a Trimethylplatinum(1V) Derivative containing an Eight-membered Chelate Ring.</xhtml:em> Journal of the Chemical Society, Dalton Transactions, 18 . pp. 2663-2665. ISSN 1477-9226</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2936/1/Dalton1992_2C_2663.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2936/1/Dalton1992_2C_2663.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />369Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="4333" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1039/DT9920002663">http://dx.doi.org/10.1039/DT9920002663</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The bidentate pyrazole-donor ligand 1,1-bis(pyrazo1-1-ylmethyl)ethene, [(pz)CH2]2C=CH2, may be synthesized in high yield on reaction of the readily obtained potassium pyrazolide with commercially available (CICH2)2C=CH2. Reaction of the ligand with [{PtMe2(SEt2)}2], followed by addition of iodomethane, gives the platinum(IV) complex fac-[PtlMe3{[(pz)CH2]2C=CH2-N,N'}]. Proton NMR and X-ray structural studies show that the eight-membered chelate ring PtNNC3NN adopts a configuration in which the pyrazole rings are in different environments, forming angles of 26.0(3) and 38.2(3) with the 'PtC2N2' mean plane. Thus, the four methylene protons are also in different environments, as are the PtMe groups trans to pyrazole groups. The eight-membered chelate ring is fluxional, undergoing inversion with DGact ~ 15 kcal mol-1 (~63 kJ mol-l) at 10 C.</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2936</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">01 Feb 2008 12:27</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">01 Feb 2008 12:27</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2936;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2936">item control page</a></p>
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