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<title>UTas ePrints - Conformational studies in palladium(IV) and platinum(IV) chemistry. Crystal structure of the l,l-bis(pyrazol-l-ethane complex fac-PtIMe3((pz)2CHMe-N,N'}</title>
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<meta content="Byers, P.K." name="eprints.creators_name" />
<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Skelton, B.W." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
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chemistry. Crystal structure of the l,l-bis(pyrazol-l-ethane complex fac-PtIMe3((pz)2CHMe-N,N'}" name="eprints.title" />
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<meta content="The reaction of iodomethane with the l,l-bis(pyrazol-1-yl)ethane complex PtMe2{(pz)2CHMe-N,N’) gives the platinum(IV) complex fac-PtIMe3((pz)2CHMe-N,N’), which has been fully characterized, by, among other means, an X-ray structural study. The analogous palladium(IV) complex has also been prepared by a similar reaction in (CD3)2C0 at - 30°C and the two complexes exhibit similar 1H NMR spectra. For the palladium(IV) species, however, reductive elimination of ethane occurs above -30°C to give PdIMe((pz)2CHMe-N,N’). The 1H NMR spectra of the platinum(IV) and palladium(IV) complexes show that they are present in one configuration in solution, and large downfield shifts of the methine CHCH3 resonance, compared with the same proton in MMe2((pz)2CHMe-N,N’), are consistent with a conformation of the six-membered chelate ring that places the methine proton adjacent to the iodine attm. The octahedral platinum(IV) complex adopts this configuration in the solid state, with I...H = 3.1 A. The 1H NMR and structural studies support earlier assignments of solution
behaviour for platinum(IV) and palladium(IV) complexes of related ligands, e.g. (pz)(py)CH, and (py)2CHMe (py = pyridin-2-yl), and confirm the influence of hydrogen...halogen interactions on 1H NMR spectra of octahedral complexes of this type." name="eprints.abstract" />
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chemistry. Crystal structure of the l,l-bis(pyrazol-l-ethane complex fac-PtIMe3((pz)2CHMe-N,N'}" name="DC.title" />
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<meta content="The reaction of iodomethane with the l,l-bis(pyrazol-1-yl)ethane complex PtMe2{(pz)2CHMe-N,N’) gives the platinum(IV) complex fac-PtIMe3((pz)2CHMe-N,N’), which has been fully characterized, by, among other means, an X-ray structural study. The analogous palladium(IV) complex has also been prepared by a similar reaction in (CD3)2C0 at - 30°C and the two complexes exhibit similar 1H NMR spectra. For the palladium(IV) species, however, reductive elimination of ethane occurs above -30°C to give PdIMe((pz)2CHMe-N,N’). The 1H NMR spectra of the platinum(IV) and palladium(IV) complexes show that they are present in one configuration in solution, and large downfield shifts of the methine CHCH3 resonance, compared with the same proton in MMe2((pz)2CHMe-N,N’), are consistent with a conformation of the six-membered chelate ring that places the methine proton adjacent to the iodine attm. The octahedral platinum(IV) complex adopts this configuration in the solid state, with I...H = 3.1 A. The 1H NMR and structural studies support earlier assignments of solution
behaviour for platinum(IV) and palladium(IV) complexes of related ligands, e.g. (pz)(py)CH, and (py)2CHMe (py = pyridin-2-yl), and confirm the influence of hydrogen...halogen interactions on 1H NMR spectra of octahedral complexes of this type." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Conformational studies in palladium(IV) and platinum(IV) chemistry. Crystal structure of the l,l-bis(pyrazol-l-ethane complex fac-PtIMe3((pz)2CHMe-N,N'}</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Byers, P.K.</span> and <span class="person_name">Canty, A.J.</span> and <span class="person_name">Skelton, B.W.</span> and <span class="person_name">White, A.H.</span> (1992) <xhtml:em>Conformational studies in palladium(IV) and platinum(IV) chemistry. Crystal structure of the l,l-bis(pyrazol-l-ethane complex fac-PtIMe3((pz)2CHMe-N,N'}.</xhtml:em> Journal of Organometallic Chemistry, 433 (1- 2). pp. 223-229. ISSN 0022-328X</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2956/1/JOMC1992_2C_223.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2956/1/JOMC1992_2C_223.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />439Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="4378" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1016/0022-328X(92)80144-M">http://dx.doi.org/10.1016/0022-328X(92)80144-M</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The reaction of iodomethane with the l,l-bis(pyrazol-1-yl)ethane complex PtMe2{(pz)2CHMe-N,N’) gives the platinum(IV) complex fac-PtIMe3((pz)2CHMe-N,N’), which has been fully characterized, by, among other means, an X-ray structural study. The analogous palladium(IV) complex has also been prepared by a similar reaction in (CD3)2C0 at - 30°C and the two complexes exhibit similar 1H NMR spectra. For the palladium(IV) species, however, reductive elimination of ethane occurs above -30°C to give PdIMe((pz)2CHMe-N,N’). The 1H NMR spectra of the platinum(IV) and palladium(IV) complexes show that they are present in one configuration in solution, and large downfield shifts of the methine CHCH3 resonance, compared with the same proton in MMe2((pz)2CHMe-N,N’), are consistent with a conformation of the six-membered chelate ring that places the methine proton adjacent to the iodine attm. The octahedral platinum(IV) complex adopts this configuration in the solid state, with I...H = 3.1 A. The 1H NMR and structural studies support earlier assignments of solution
behaviour for platinum(IV) and palladium(IV) complexes of related ligands, e.g. (pz)(py)CH, and (py)2CHMe (py = pyridin-2-yl), and confirm the influence of hydrogen...halogen interactions on 1H NMR spectra of octahedral complexes of this type.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Additional Information:</th><td valign="top" class="ep_row">The definitive version is available at http://www.sciencedirect.com
</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2956</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">05 Feb 2008 08:35</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">05 Feb 2008 08:35</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2956;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2956">item control page</a></p>
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