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<title>UTas ePrints - Crystal and Molecular Structure of the 2:1 Adduct of Bis(pentafluorophenyl)mercury(II) and Bis(diphenylarsino)methane</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Gatehouse, B.M." name="eprints.creators_name" />
<meta content="allan.canty@utas.edu.au" name="eprints.creators_id" />
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<meta content="The title compound crystallizes in the monoclinic system with a = 14.07, b = 17.34, c = 19-33 8, beta = 91" 3'.
Z = 4, and space-group C2/c. The structure was solved by conventional Patterson and Fourier methods and refined
by least-squares techniques to R 0.9 for 1218 independent reflections. The compound has a two-fold axis about the methylene carbon atom of the diarsine moiety. Each mercury atom has one arsenic atom within the sum of van der Waals radii from it, and there is a T-shaped distribution of two C6F5 groups and the arsenic atom about mercury with a Hg...As distance of 3.40 +/- 0.02 A and C-Hg-C angle of 173 +/- 4'. X-Ray powder diffraction photographs
indicate that the compound [(C6F5)2Hg],Ph2PCH2PPh2 has the same structure." name="eprints.abstract" />
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J. Inorg. Nuclear Chem., 1964, 26, 203.
5 A. J. Canty and G. B. Deacon, Austral. J. Chem., 1971, 24,
489.
A. J. Canty and B. M. Gatehouse, Chem. Comm., 1971, 443.
7 N. R. Kunchur and M. Mathew, Chem. Comm., 1966, 71.
L. Pauling, ' The Nature of the Chemical Bond,' 3rd edn.,
Cornell, University Press, Ithaca, New York.
G. Dwyer, D. C. Goodall, R. H. B. Mais, H. M. Powell,
and L. M. Venanzi, J. Chem. Soc. ('4), 1966, 1110.
10 R. S. McEwen and G. A. Sim, J. Chem. SOC. (A), 1969, 1897.
l1 J. T. Mague, Inorg. Chem., 1969, 8, 1975." name="eprints.referencetext" />
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<meta content="The title compound crystallizes in the monoclinic system with a = 14.07, b = 17.34, c = 19-33 8, beta = 91" 3'.
Z = 4, and space-group C2/c. The structure was solved by conventional Patterson and Fourier methods and refined
by least-squares techniques to R 0.9 for 1218 independent reflections. The compound has a two-fold axis about the methylene carbon atom of the diarsine moiety. Each mercury atom has one arsenic atom within the sum of van der Waals radii from it, and there is a T-shaped distribution of two C6F5 groups and the arsenic atom about mercury with a Hg...As distance of 3.40 +/- 0.02 A and C-Hg-C angle of 173 +/- 4'. X-Ray powder diffraction photographs
indicate that the compound [(C6F5)2Hg],Ph2PCH2PPh2 has the same structure." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Crystal and Molecular Structure of the 2:1 Adduct of Bis(pentafluorophenyl)mercury(II) and Bis(diphenylarsino)methane</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Gatehouse, B.M.</span> (1972) <xhtml:em>Crystal and Molecular Structure of the 2:1 Adduct of Bis(pentafluorophenyl)mercury(II) and Bis(diphenylarsino)methane.</xhtml:em> Journal of the Chemical Society, Dalton Transactions, 4 . pp. 511-514. ISSN 1477-9226</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2855/1/Dalton1972_2C_511.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2855/1/Dalton1972_2C_511.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />503Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="4076" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1039/DT9720000511">http://dx.doi.org/10.1039/DT9720000511</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The title compound crystallizes in the monoclinic system with a = 14.07, b = 17.34, c = 19-33 8, beta = 91" 3'.
Z = 4, and space-group C2/c. The structure was solved by conventional Patterson and Fourier methods and refined
by least-squares techniques to R 0.9 for 1218 independent reflections. The compound has a two-fold axis about the methylene carbon atom of the diarsine moiety. Each mercury atom has one arsenic atom within the sum of van der Waals radii from it, and there is a T-shaped distribution of two C6F5 groups and the arsenic atom about mercury with a Hg...As distance of 3.40 +/- 0.02 A and C-Hg-C angle of 173 +/- 4'. X-Ray powder diffraction photographs
indicate that the compound [(C6F5)2Hg],Ph2PCH2PPh2 has the same structure.</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2855</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">14 Jan 2008 10:14</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">14 Jan 2008 10:14</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2855;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2855">item control page</a></p>
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