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<title>UTas ePrints - Organo(organooxo)mercury(II) chemistry — Synthesis and structure of methyl(phenoxo)mercury(II)</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Devereux, J.W." name="eprints.creators_name" />
<meta content="Skelton, B.W." name="eprints.creators_name" />
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<meta content="Methyl(phenoxo)mercury(II), i.e. methylmercury phenoxide, may be obtained from the reaction of methyl(chloro)mercury(II) with silver(I)
oxide, followed by addition of phenol. The dominant motif of the structure is a pair of independent MeHgOPh aggregates (Hg—C,O 2.05(2) Å, 2.06(1) Å (x2); C-Hg-O 176.6(5)°, 176.3(5)°) loosely associated about a quasi-inversion
centre by Hg···O interactions (2.702(9) Å, 2.719(9) Å) to form a dimer (Hg-O-Hg′ 106.0(4)°, 106.5(4)°; O-Hg-O′ 73.0(3)°, 72.6(3)°), the dimer stacking up the short crystallographic c axis (= 6.914(1) Å) at spacings c/2. Vibrational spectroscopic studies are insensitive to the associative interactions." name="eprints.abstract" />
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<meta content="1. J.L. Wardell. In Comprehensive organometallic chemistry.
Vol. 1. Edited by G. Wilkinson, F.G.A. Stone, and E.W. Abel.
Pergamon Press, Oxford. 1982. p. 863.
2. J.S. Casas, M.S. García-Tasende, and J. Sordo. Coord. Chem.
Rev. 193–195, 283 (1999).
3. L.G. Kuz′mina, N.G. Bokii, Y.T. Struchkov, D.N. Kravtsov,
and L.G. Golovchenko. Zh. Strukt. Khim. 14, 508 (1973).
4. D.C. Bradley, R.C. Mehrotra, I.P. Rothwell, and A. Singh.
Alkoxo and aryloxo derivatives of metals. Academic Press,
San Diego. 2001.
5. G. Dittmar and E. Hellner. Angew. Chem. 81, 707 (1969).
6. A.J. Canty and J.W. Devereux. Spectrochim. Acta, 36A, 495
(1980).
7. A.J. Bloodworth. J. Chem. Soc. C, 2051 (1970).
8. G. Holan. Tetrahedron Lett. 1985 (1966).
9. H. Schmidbaur and F. Schindler. Angew. Chem. Int. Ed. Engl.
4, 876 (1965).
10. A.J. Canty and B.M. Gatehouse. J. Chem. Soc. Dalton Trans.
2018 (1976).
11. Y.S. Wong, P.C. Chieh, and A.J. Carty. Can. J. Chem. 51, 2597
(1973).
12. A.J. Carty, S.F. Malone, N.J. Taylor, and A.J. Canty. J. Inorg.
Biochem. 18, 291 (1983).
13. L.F. Sytsma and R.J. Kline. J. Organomet. Chem. 54, 15 (1973).
14. L. Pauling. The nature of the chemical bond. 3rd ed. Cornell
University Press, Ithaca, New York. 1960. p. 260.
15. A.J. Canty and G.B. Deacon. Inorg. Chim. Acta, 45, L225
(1980).
16. S.R. Hall, D.J. du Boulay, and R. Olthof-Hazekamp. The
XTAL 3.7 system [computer program]. University of Western
Australia, Crawley, Australia. 2001.
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<meta content="Devereux, J.W." name="DC.creator" />
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<meta content="Methyl(phenoxo)mercury(II), i.e. methylmercury phenoxide, may be obtained from the reaction of methyl(chloro)mercury(II) with silver(I)
oxide, followed by addition of phenol. The dominant motif of the structure is a pair of independent MeHgOPh aggregates (Hg—C,O 2.05(2) Å, 2.06(1) Å (x2); C-Hg-O 176.6(5)°, 176.3(5)°) loosely associated about a quasi-inversion
centre by Hg···O interactions (2.702(9) Å, 2.719(9) Å) to form a dimer (Hg-O-Hg′ 106.0(4)°, 106.5(4)°; O-Hg-O′ 73.0(3)°, 72.6(3)°), the dimer stacking up the short crystallographic c axis (= 6.914(1) Å) at spacings c/2. Vibrational spectroscopic studies are insensitive to the associative interactions." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Organo(organooxo)mercury(II) chemistry — Synthesis and structure of methyl(phenoxo)mercury(II)</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Devereux, J.W.</span> and <span class="person_name">Skelton, B.W.</span> and <span class="person_name">White, A.H.</span> (2006) <xhtml:em>Organo(organooxo)mercury(II) chemistry — Synthesis and structure of methyl(phenoxo)mercury(II).</xhtml:em> Canadian Journal of Chemistry, 84 (2). pp. 77-80. ISSN 0008-4042</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2807/1/CanJChemoc_5B1_5D.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2807/1/CanJChemoc_5B1_5D.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />178Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="3829" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1139/V05-219">http://dx.doi.org/10.1139/V05-219</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">Methyl(phenoxo)mercury(II), i.e. methylmercury phenoxide, may be obtained from the reaction of methyl(chloro)mercury(II) with silver(I)
oxide, followed by addition of phenol. The dominant motif of the structure is a pair of independent MeHgOPh aggregates (Hg—C,O 2.05(2) Å, 2.06(1) Å (x2); C-Hg-O 176.6(5)°, 176.3(5)°) loosely associated about a quasi-inversion
centre by Hg···O interactions (2.702(9) Å, 2.719(9) Å) to form a dimer (Hg-O-Hg′ 106.0(4)°, 106.5(4)°; O-Hg-O′ 73.0(3)°, 72.6(3)°), the dimer stacking up the short crystallographic c axis (= 6.914(1) Å) at spacings c/2. Vibrational spectroscopic studies are insensitive to the associative interactions.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Keywords:</th><td valign="top" class="ep_row">mercury, methylmercury, organomercury, structure, aryloxide, phenoxide.</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2807</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">04 Jan 2008 11:43</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">09 Jan 2008 02:30</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2807;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2807">item control page</a></p>
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