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<meta content="Coordination complexes and organometallic complexes of palladium and platinum with polydentate ligands containing pyrazole groups and related ligands: an electrospray mass spectrometric study
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<meta content="Electrospray mass spectra have been obtained from methanol solution for a wide variety of organometallic compounds of palladium(IV,II) and platinum(IV) containing polydentate nitrogen donor ligands. In almost every case the intact ion was observed as the base peak, and often as the only peak, at low ion source energies emphasising the very soft nature of the transfer of ions from solution to the gas phase. Daughter ions were generated either by collisional activated decompositions involving solvent molecules within the ion source as the source energy was increased, or alternatively by tandem mass spectrometry using argon as the collision gas. The palladium(IV) complexes all undergo very facile reductive elimination of two methyl groups, as expected for palladium(IV) complexes. In contrast, platinum(IV) compounds retain their organ groups at low ion source energies." name="eprints.abstract" />
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T.J. Cardwell, R. Colton, N. Lambropoulos, J.C. Traeger and
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A.J. Canty, R. Colton and I.M. Thomas, .I. Organomet. Chem.,
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and A.H. White, J. Chem. Sot., Dalton Trans., (1986) 645.
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<meta content="Electrospray mass spectra have been obtained from methanol solution for a wide variety of organometallic compounds of palladium(IV,II) and platinum(IV) containing polydentate nitrogen donor ligands. In almost every case the intact ion was observed as the base peak, and often as the only peak, at low ion source energies emphasising the very soft nature of the transfer of ions from solution to the gas phase. Daughter ions were generated either by collisional activated decompositions involving solvent molecules within the ion source as the source energy was increased, or alternatively by tandem mass spectrometry using argon as the collision gas. The palladium(IV) complexes all undergo very facile reductive elimination of two methyl groups, as expected for palladium(IV) complexes. In contrast, platinum(IV) compounds retain their organ groups at low ion source energies." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Coordination complexes and organometallic complexes of palladium and platinum with polydentate ligands containing pyrazole groups and related ligands: an electrospray mass spectrometric study</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Traill, P.R.</span> and <span class="person_name">Colton, R.</span> and <span class="person_name">Thomas, I.M.</span> (1993) <xhtml:em>Coordination complexes and organometallic complexes of palladium and platinum with polydentate ligands containing pyrazole groups and related ligands: an electrospray mass spectrometric study.</xhtml:em> Inorganica Chimica Acta, 210 . pp. 91-97. ISSN 1387-7003</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2811/1/ICA1993_2C_91.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2811/1/ICA1993_2C_91.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />723Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="3838" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">Electrospray mass spectra have been obtained from methanol solution for a wide variety of organometallic compounds of palladium(IV,II) and platinum(IV) containing polydentate nitrogen donor ligands. In almost every case the intact ion was observed as the base peak, and often as the only peak, at low ion source energies emphasising the very soft nature of the transfer of ions from solution to the gas phase. Daughter ions were generated either by collisional activated decompositions involving solvent molecules within the ion source as the source energy was increased, or alternatively by tandem mass spectrometry using argon as the collision gas. The palladium(IV) complexes all undergo very facile reductive elimination of two methyl groups, as expected for palladium(IV) complexes. In contrast, platinum(IV) compounds retain their organ groups at low ion source energies.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Additional Information:</th><td valign="top" class="ep_row">The definitive version is available at http://www.sciencedirect.com
</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/250200.html">250000 Chemical Sciences > 250200 Inorganic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2811</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">04 Jan 2008 13:50</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">18 Jan 2008 13:30</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2811;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2811">item control page</a></p>
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