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<title>UTas ePrints - Coordination Chemistry of Methylmercury(II) with Flexible Tripod Ligands Containing Pyridyl and N-Methylimidazolyl Groups, Including the Crystal Structure of [Bis(N-methylimidazol-2-y1)(pyridin-2-yl)methanol-N,N’,N’]methylmercury(II) Nitrate, [MeHg(py(N-MeIm)2COH)]N03</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Patrick, J.M." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
<meta content="allan.canty@utas.edu.au" name="eprints.creators_id" />
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<meta content="Coordination Chemistry of Methylmercury(II) with Flexible Tripod Ligands Containing Pyridyl and N-Methylimidazolyl Groups, Including the Crystal Structure of [Bis(N-methylimidazol-2-y1)(pyridin-2-yl)methanol-N,N’,N’]methylmercury(II) Nitrate, [MeHg(py(N-MeIm)2COH)]N03" name="eprints.title" />
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<meta content="The ligand is present as a tridentate, based on one strong
Hg-N(1’) (N-MeIm) bond, 2.12 (1) A, and two weak Hg...N
interactions of 2.58 (1) A (N-MeIm) and 2.89 (1) A (py). As
expected for the presence of weak Hg...N interactions, the
C(1)-Hg-N(1’) angle is not far removed from linearity, 170.5(7)O, with the Hg...N interactions opposite this angle. Although the weak interactions are well short of van der Waals contact (ca. 3.23 A), they are clearly weak since the mercury atom lies 1.589 A above the mean plane of the N-MeIm ring and 0.456 A above the mean plane of the pyridine ring, compared with 0.304 A for the strongly bound N-MeIm ring. Although the hydroxyl hydrogen could not be confidently located, a close contact is observed to the nitrate ion, 0-(H)...O(1) being 2.71 (1) A; no other 0...O distances <3.2 A were observed." name="eprints.abstract" />
<meta content="1984" name="eprints.date" />
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<meta content="The ligand is present as a tridentate, based on one strong
Hg-N(1’) (N-MeIm) bond, 2.12 (1) A, and two weak Hg...N
interactions of 2.58 (1) A (N-MeIm) and 2.89 (1) A (py). As
expected for the presence of weak Hg...N interactions, the
C(1)-Hg-N(1’) angle is not far removed from linearity, 170.5(7)O, with the Hg...N interactions opposite this angle. Although the weak interactions are well short of van der Waals contact (ca. 3.23 A), they are clearly weak since the mercury atom lies 1.589 A above the mean plane of the N-MeIm ring and 0.456 A above the mean plane of the pyridine ring, compared with 0.304 A for the strongly bound N-MeIm ring. Although the hydroxyl hydrogen could not be confidently located, a close contact is observed to the nitrate ion, 0-(H)...O(1) being 2.71 (1) A; no other 0...O distances <3.2 A were observed." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Coordination Chemistry of Methylmercury(II) with Flexible Tripod Ligands Containing Pyridyl and N-Methylimidazolyl Groups, Including the Crystal Structure of [Bis(N-methylimidazol-2-y1)(pyridin-2-yl)methanol-N,N’,N’]methylmercury(II) Nitrate, [MeHg(py(N-MeIm)2COH)]N03</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Patrick, J.M.</span> and <span class="person_name">White, A.H.</span> (1984) <xhtml:em>Coordination Chemistry of Methylmercury(II) with Flexible Tripod Ligands Containing Pyridyl and N-Methylimidazolyl Groups, Including the Crystal Structure of [Bis(N-methylimidazol-2-y1)(pyridin-2-yl)methanol-N,N’,N’]methylmercury(II) Nitrate, [MeHg(py(N-MeIm)2COH)]N03.</xhtml:em> Inorganic Chemistry, 23 (23). pp. 3827-3830. ISSN 0020-1669</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2951/1/IC1984_2C_3827.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2951/1/IC1984_2C_3827.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />542Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="4332" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1021/ic00191a032">http://dx.doi.org/10.1021/ic00191a032</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The ligand is present as a tridentate, based on one strong
Hg-N(1’) (N-MeIm) bond, 2.12 (1) A, and two weak Hg...N
interactions of 2.58 (1) A (N-MeIm) and 2.89 (1) A (py). As
expected for the presence of weak Hg...N interactions, the
C(1)-Hg-N(1’) angle is not far removed from linearity, 170.5(7)O, with the Hg...N interactions opposite this angle. Although the weak interactions are well short of van der Waals contact (ca. 3.23 A), they are clearly weak since the mercury atom lies 1.589 A above the mean plane of the N-MeIm ring and 0.456 A above the mean plane of the pyridine ring, compared with 0.304 A for the strongly bound N-MeIm ring. Although the hydroxyl hydrogen could not be confidently located, a close contact is observed to the nitrate ion, 0-(H)...O(1) being 2.71 (1) A; no other 0...O distances <3.2 A were observed.</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2951</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">01 Feb 2008 12:04</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">01 Feb 2008 12:04</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2951;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2951">item control page</a></p>
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