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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Deverell, J.A." name="eprints.creators_name" />
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<meta content="A solid macroporous monolith is shown to be a suitable substrate for anchoring a palladium complex to obtain a continuous porous material suitable for conducting flow-through catalysis in capillary microreactors. The monolith for this study was GMA-co-EDMA [poly(glycidyl
methacrylate-co-ethylene dimethacrylate)] in fused silica capillaries (250 micrometre internal diameter). Immobilisation of ligand was achieved by passing a solution of 5-hydroxy-1,10-phenanthroline, and palladium(II) was added. Suzuki-Miyaura catalysis was studied. The excellent flow-through properties, firm attachment
to capillary walls, and robustness of the capillary systems
for catalysis demonstrated after continuous reaction for four days indicate that this approach is suitable for further development of capillary-based microreactors that are suitable for continuous flow processes and parallel synthesis." name="eprints.abstract" />
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methacrylate-co-ethylene dimethacrylate)] in fused silica capillaries (250 micrometre internal diameter). Immobilisation of ligand was achieved by passing a solution of 5-hydroxy-1,10-phenanthroline, and palladium(II) was added. Suzuki-Miyaura catalysis was studied. The excellent flow-through properties, firm attachment
to capillary walls, and robustness of the capillary systems
for catalysis demonstrated after continuous reaction for four days indicate that this approach is suitable for further development of capillary-based microreactors that are suitable for continuous flow processes and parallel synthesis." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Macroporous monolith supports for continuous flow capillary microreactors</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Bolton, K.F.</span> and <span class="person_name">Canty, A.J.</span> and <span class="person_name">Deverell, J.A.</span> and <span class="person_name">Guijt, R.M.</span> and <span class="person_name">Hilder, E.F.</span> and <span class="person_name">Rodemann, T.</span> and <span class="person_name">Smith, J.A.</span> (2006) <xhtml:em>Macroporous monolith supports for continuous flow capillary microreactors.</xhtml:em> Tetrahedron Letters, 47 (52). pp. 9321-9324. ISSN 0040-4039</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/3082/1/TetLett2006%2C_9321.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/3082/1/TetLett2006%2C_9321.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />220Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="4229" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1016/j.tetlet.2006.10.113">http://dx.doi.org/10.1016/j.tetlet.2006.10.113</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">A solid macroporous monolith is shown to be a suitable substrate for anchoring a palladium complex to obtain a continuous porous material suitable for conducting flow-through catalysis in capillary microreactors. The monolith for this study was GMA-co-EDMA [poly(glycidyl
methacrylate-co-ethylene dimethacrylate)] in fused silica capillaries (250 micrometre internal diameter). Immobilisation of ligand was achieved by passing a solution of 5-hydroxy-1,10-phenanthroline, and palladium(II) was added. Suzuki-Miyaura catalysis was studied. The excellent flow-through properties, firm attachment
to capillary walls, and robustness of the capillary systems
for catalysis demonstrated after continuous reaction for four days indicate that this approach is suitable for further development of capillary-based microreactors that are suitable for continuous flow processes and parallel synthesis.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Additional Information:</th><td valign="top" class="ep_row">The definitive version is available at http://www.sciencedirect.com
</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/250102.html">250000 Chemical Sciences > 250100 Physical Chemistry (incl. Structural) > 250102 Chemistry of Catalysis</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">3082</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">23 Jan 2008 10:00</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">23 Jan 2008 10:00</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=3082;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=3082">item control page</a></p>
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