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<title>UTas ePrints - Crystal and Molecular Structure of Polymeric MeSHgO2CMe and MeSHgO2CMe,C5H5N and the Tetranuclear Complex (ButS)-4C14Hg4(C5H5N)2</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Raston, C.L." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
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<meta content="Crystal and Molecular Structure of Polymeric MeSHgO2CMe and MeSHgO2CMe,C5H5N and the Tetranuclear Complex (ButS)-4C14Hg4(C5H5N)2" name="eprints.title" />
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<meta content="Crystals of methanethiolatomercury(II) acetate are monoclinic, P 21/c, with a 5.292(2), b 15.912(7), c 7.O86(2) A, beta 92.96(3), Z 4, and its pyridine complex MeSHgO2CMe,C5H5N is monoclinic, P21/n, with a 10.093(3), b 7.026(2), c 15.350(5) A, beta 105.01(3), Z 4 . Both structures are based on a polymeric chain (-Hg-SMe-)n with coordinated acetate groups. In MeSHg02CMe the chains are
linked into sheets by bridging acetate groups, and in the pyridine complex the chains are isolated with pyridine and acetate coordination at each mercury. Crystals of
(ButS)4CI4Hg4(C5H5N)2 are triclinic, P1 bar, with a 14.399(6), b 9.893(6), c 9.597(5) A, alpha 121.82(1), beta 102.52(4), gamma 102.94(4), and Z 1. The structure is based on a tetranuclear grouping of mercury atoms bridged by chloride and thiolate species and centrosymmetric about the origin. There are two mercury environments 'Hg(mu-SBut)2ClN' and Hg(mu-SBut)2(mu-Cl)2' with the dichloro bridge linking two equivalent mercury atoms on opposite sides of an (-Hg-SBut-)4 ring." name="eprints.abstract" />
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Cromer, D. T., and Mann, J. B., Acta Crystallogr., Sect. A, 1968, 24, 321.
Cromer, D. T., and Liberman, D., J. Chem. Phys., 1970,63, 1891.
Stewart, R. F., Davidson, E. R., and Simpson, W. T., J. Chem. Phys., 1965, 42, 3175.
'The X-RAY System-Version of March, 1976' Technical Report TR-192, Computer Science Center,
University of Maryland, U.S.A.
Puff, H., Sievers, R., and Elsner, G., Z. Anorg. Allg. Chem., 1975,413, 37.
' E.g. Brotherton, P. D., and White, A. H., J. Chem. Soc., Dalton Trans., 1973,2698, and references
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<meta content="Crystals of methanethiolatomercury(II) acetate are monoclinic, P 21/c, with a 5.292(2), b 15.912(7), c 7.O86(2) A, beta 92.96(3), Z 4, and its pyridine complex MeSHgO2CMe,C5H5N is monoclinic, P21/n, with a 10.093(3), b 7.026(2), c 15.350(5) A, beta 105.01(3), Z 4 . Both structures are based on a polymeric chain (-Hg-SMe-)n with coordinated acetate groups. In MeSHg02CMe the chains are
linked into sheets by bridging acetate groups, and in the pyridine complex the chains are isolated with pyridine and acetate coordination at each mercury. Crystals of
(ButS)4CI4Hg4(C5H5N)2 are triclinic, P1 bar, with a 14.399(6), b 9.893(6), c 9.597(5) A, alpha 121.82(1), beta 102.52(4), gamma 102.94(4), and Z 1. The structure is based on a tetranuclear grouping of mercury atoms bridged by chloride and thiolate species and centrosymmetric about the origin. There are two mercury environments 'Hg(mu-SBut)2ClN' and Hg(mu-SBut)2(mu-Cl)2' with the dichloro bridge linking two equivalent mercury atoms on opposite sides of an (-Hg-SBut-)4 ring." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Crystal and Molecular Structure of Polymeric MeSHgO2CMe and MeSHgO2CMe,C5H5N and the Tetranuclear Complex (ButS)-4C14Hg4(C5H5N)2</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Raston, C.L.</span> and <span class="person_name">White, A.H.</span> (1978) <xhtml:em>Crystal and Molecular Structure of Polymeric MeSHgO2CMe and MeSHgO2CMe,C5H5N and the Tetranuclear Complex (ButS)-4C14Hg4(C5H5N)2.</xhtml:em> Australian Journal of Chemistry, 31 (3). pp. 677-684. ISSN 0004-9425</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2826/1/AJC1978_2C_677.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2826/1/AJC1978_2C_677.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />297Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="4030" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://www.publish.csiro.au/paper/CH9780677.htm">http://www.publish.csiro.au/paper/CH9780677.htm</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">Crystals of methanethiolatomercury(II) acetate are monoclinic, P 21/c, with a 5.292(2), b 15.912(7), c 7.O86(2) A, beta 92.96(3), Z 4, and its pyridine complex MeSHgO2CMe,C5H5N is monoclinic, P21/n, with a 10.093(3), b 7.026(2), c 15.350(5) A, beta 105.01(3), Z 4 . Both structures are based on a polymeric chain (-Hg-SMe-)n with coordinated acetate groups. In MeSHg02CMe the chains are
linked into sheets by bridging acetate groups, and in the pyridine complex the chains are isolated with pyridine and acetate coordination at each mercury. Crystals of
(ButS)4CI4Hg4(C5H5N)2 are triclinic, P1 bar, with a 14.399(6), b 9.893(6), c 9.597(5) A, alpha 121.82(1), beta 102.52(4), gamma 102.94(4), and Z 1. The structure is based on a tetranuclear grouping of mercury atoms bridged by chloride and thiolate species and centrosymmetric about the origin. There are two mercury environments 'Hg(mu-SBut)2ClN' and Hg(mu-SBut)2(mu-Cl)2' with the dichloro bridge linking two equivalent mercury atoms on opposite sides of an (-Hg-SBut-)4 ring.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/250200.html">250000 Chemical Sciences > 250200 Inorganic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2826</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">11 Jan 2008 11:38</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">11 Jan 2008 11:38</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2826;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2826">item control page</a></p>
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