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<title>UTas ePrints - Synthesis and Spectroscopic Studies of RSHg(II) Complexes, Including Complexes of ButSHgX (X = C1, Br) and RSHgO2CMe (R = Me, Et) with Pyridine</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Kishimoto, R." name="eprints.creators_name" />
<meta content="Tyson, R.K." name="eprints.creators_name" />
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<meta content="The complexes RSHgX (R = Et, But; X = C1, Br) may be prepared by reaction of the alkanethiol with HgX2 in ethanol, and the 2-methylpropane-2-thiolates crystallize from pyridine as (ButSHgC1)2C5H5N and ButSHgBr.C5H5N. The complexes RSHgO2CMe (R = Me, Et) may be prepared by
reaction of mercuric acetate with Hg(SR)2 in water, and form crystalline RSHgO2CMe.C5H5N when dissolved in pyridine. Infrared and Raman spectra indicate coordination of pyridine in the pyridinates. Mercury-sulfur stretching vibrations of RSHg02CMe (R = Me, Et, Pr, Bu) are discussed." name="eprints.abstract" />
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<meta content="The complexes RSHgX (R = Et, But; X = C1, Br) may be prepared by reaction of the alkanethiol with HgX2 in ethanol, and the 2-methylpropane-2-thiolates crystallize from pyridine as (ButSHgC1)2C5H5N and ButSHgBr.C5H5N. The complexes RSHgO2CMe (R = Me, Et) may be prepared by
reaction of mercuric acetate with Hg(SR)2 in water, and form crystalline RSHgO2CMe.C5H5N when dissolved in pyridine. Infrared and Raman spectra indicate coordination of pyridine in the pyridinates. Mercury-sulfur stretching vibrations of RSHg02CMe (R = Me, Et, Pr, Bu) are discussed." name="DC.description" />
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<h1 class="ep_tm_pagetitle">Synthesis and Spectroscopic Studies of RSHg(II) Complexes, Including Complexes of ButSHgX (X = C1, Br) and RSHgO2CMe (R = Me, Et) with Pyridine</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Kishimoto, R.</span> and <span class="person_name">Tyson, R.K.</span> (1978) <xhtml:em>Synthesis and Spectroscopic Studies of RSHg(II) Complexes, Including Complexes of ButSHgX (X = C1, Br) and RSHgO2CMe (R = Me, Et) with Pyridine.</xhtml:em> Australian Journal of Chemistry, 31 (3). pp. 671-676. ISSN 0004-9425</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2925/1/AJC1978_2C_671.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2925/1/AJC1978_2C_671.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />332Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="4311" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://www.publish.csiro.au/nid/51/paper/CH9780671.htm">http://www.publish.csiro.au/nid/51/paper/CH9780671.htm</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The complexes RSHgX (R = Et, But; X = C1, Br) may be prepared by reaction of the alkanethiol with HgX2 in ethanol, and the 2-methylpropane-2-thiolates crystallize from pyridine as (ButSHgC1)2C5H5N and ButSHgBr.C5H5N. The complexes RSHgO2CMe (R = Me, Et) may be prepared by
reaction of mercuric acetate with Hg(SR)2 in water, and form crystalline RSHgO2CMe.C5H5N when dissolved in pyridine. Infrared and Raman spectra indicate coordination of pyridine in the pyridinates. Mercury-sulfur stretching vibrations of RSHg02CMe (R = Me, Et, Pr, Bu) are discussed.</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/250200.html">250000 Chemical Sciences > 250200 Inorganic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2925</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">01 Feb 2008 08:35</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">01 Feb 2008 08:35</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2925;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2925">item control page</a></p>
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