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<title>UTas ePrints - Platinum-Tin Bonded Complexes, Including a Structural Analysis of the Octahedral Tris(pyrazol-1-yl)borate Complex Pt(SnMe3)Me2{(pz)3BH-N,N',N"}</title>
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<meta content="Skelton, B.W." name="eprints.creators_name" />
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<meta content="The platinum(II) complex K[PtMe2{(pz)3BH-N,N'}] reacts with SnCl2Me2 to form Pt(SnClMe2)Me2{(pz)3BH-N,N',N"} ([(pz)3BH]- =tris(pyrazol-1-yl)borate). The closely related complex Pt(SnMe3)Me2{(pz)3BH-N,N',N"} has distorted octahedral geometry for platinum with Pt-Sn 2.5727(8) A. The Pt-N distance trans to the SnMe3 group [2.237(7) A] is longer than those trans to the Me groups
[2.127(7) and 2.131(6) A], indicating for the trimethylstannyl group a trans influence which is higher
than that for the methyl group." name="eprints.abstract" />
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1 Kuyper, J., Inorg. Chem., 1977, 16, 2171.
2 Almeida, J. F., Azizian, H., Eaborn, C., and Pidcock, A.,
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van der Sluis, P., Spek, A. L., and van Koten, G., J. Am.
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97, 1735.
12 Canty, A. J., and Jin, H., J. Organomet. Chem., 1998, 565,
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13 Canty, A. J., Fritsche, S. D., Jin, H., Patel, J., Skelton, B.
W., and White, A. H., Organometallics, 1997, 16, 2175.
14 Canty, A. J., Dedieu, A., Jin, H., Milet, A., Skelton, B.
W., Tro¯menko, S., and White, A. H., Inorg. Chim. Acta,
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K., Transition Met. Chem., 1976, 1, 199.
17 Hall, S. R., King, G. S. D., and Stewart, J. M., (Eds)
\The Xtal 3.4 User's Manual" (The University of Western
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y" name="eprints.referencetext" />
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<meta content="The platinum(II) complex K[PtMe2{(pz)3BH-N,N'}] reacts with SnCl2Me2 to form Pt(SnClMe2)Me2{(pz)3BH-N,N',N"} ([(pz)3BH]- =tris(pyrazol-1-yl)borate). The closely related complex Pt(SnMe3)Me2{(pz)3BH-N,N',N"} has distorted octahedral geometry for platinum with Pt-Sn 2.5727(8) A. The Pt-N distance trans to the SnMe3 group [2.237(7) A] is longer than those trans to the Me groups
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<h1 class="ep_tm_pagetitle">Platinum-Tin Bonded Complexes, Including a Structural Analysis of the Octahedral Tris(pyrazol-1-yl)borate Complex Pt(SnMe3)Me2{(pz)3BH-N,N',N"}</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Jin, H.</span> and <span class="person_name">Skelton, B.W.</span> and <span class="person_name">White, A.H.</span> (1999) <xhtml:em>Platinum-Tin Bonded Complexes, Including a Structural Analysis of the Octahedral Tris(pyrazol-1-yl)borate Complex Pt(SnMe3)Me2{(pz)3BH-N,N',N"}.</xhtml:em> Australian Journal of Chemistry, 52 (5). pp. 417-419. ISSN 0004-9425</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2879/1/AJC1999_2C_417.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2879/1/AJC1999_2C_417.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />149Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="4111" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://www.publish.csiro.au/nid/51/paper/CH98166.htm">http://www.publish.csiro.au/nid/51/paper/CH98166.htm</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The platinum(II) complex K[PtMe2{(pz)3BH-N,N'}] reacts with SnCl2Me2 to form Pt(SnClMe2)Me2{(pz)3BH-N,N',N"} ([(pz)3BH]- =tris(pyrazol-1-yl)borate). The closely related complex Pt(SnMe3)Me2{(pz)3BH-N,N',N"} has distorted octahedral geometry for platinum with Pt-Sn 2.5727(8) A. The Pt-N distance trans to the SnMe3 group [2.237(7) A] is longer than those trans to the Me groups
[2.127(7) and 2.131(6) A], indicating for the trimethylstannyl group a trans influence which is higher
than that for the methyl group.</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2879</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">16 Jan 2008 09:11</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">16 Jan 2008 09:11</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2879;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2879">item control page</a></p>
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