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<title>UTas ePrints - Interaction of Palladium(II) Acetate with Substituted Pyridines, including a Cyclometallation Reaction and the Structure of [Pd{meso-[(py)PhMeC]2C5H3N}(02CMe)][02CMe].3H2O</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Minchin, N.J." name="eprints.creators_name" />
<meta content="Skelton, B.W." name="eprints.creators_name" />
<meta content="White, A.H." name="eprints.creators_name" />
<meta content="allan.canty@utas.edu.au" name="eprints.creators_id" />
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<meta content="2008-01-29T02:51:24Z" name="eprints.datestamp" />
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<meta content="Interaction of Palladium(II) Acetate with Substituted Pyridines, including a Cyclometallation Reaction and the Structure of [Pd{meso-[(py)PhMeC]2C5H3N}(02CMe)][02CMe].3H2O" name="eprints.title" />
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<meta content="The reactivity of meso- and rac- diastereoisomers of 2,6-bis[l-phenyl-1-(pyridin-2-yl)ethyl]pyridine {[(py)PhMeC]2C5H3N}, 2,6-bis[l,l-bis(pyridin-2-yl)ethyl]pyridine {[(py)2MeC]2C5H3N}, and the pyridin-2-ylmethanes (py)2Ph3-nCH (n = 1-3), (py)nCH4-n, (n = 2 or 3), and (py)3PhC toward
palladium(II) acetate in refluxing glacial acetic acid and at ambient temperature in organic solvents has been investigated. The nitrogen donor ligands form co-ordination derivatives in organic solvents. All except alpha-phenyl-alpha-(pyridin-2-yl)toluene [(py)Ph2CH] form identical complexes in glacial acetic acid, with (py)Ph2CH undergoing cyclometallation to form [{Pd[(py)PhHCC6H4](mu-
O2CMe)}2]. meso-[(py)PhMeC]2C5H3N, which binds as a tripodal tridentate ligand to methylmercury(II), has been shown by a single crystal X-ray study to act as a planar tridentate ligand to palladium(II) in [Pd{meso-[(pyPhMeC]2C5H3N}(O2CMe)][O2CMe].3H2O with square-planar co-ordination being completed by a unidentate acetate group. Syntheses of the new ligand [(py)2MeC]2C5H3N, with five pyridine donor groups, and alpha,alpha,alpha-tris(pyridin-2-y1)toluene [(py)3PhC] are described." name="eprints.abstract" />
<meta content="1986" name="eprints.date" />
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<meta content="Canty, A.J. and Minchin, N.J. and Skelton, B.W. and White, A.H. (1986) Interaction of Palladium(II) Acetate with Substituted Pyridines, including a Cyclometallation Reaction and the Structure of [Pd{meso-[(py)PhMeC]2C5H3N}(02CMe)][02CMe].3H2O. Journal of the Chemical Society, Dalton Transactions, 10 . pp. 2205-2210. ISSN 1477-9226" name="eprints.citation" />
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<meta content="Canty, A.J." name="DC.creator" />
<meta content="Minchin, N.J." name="DC.creator" />
<meta content="Skelton, B.W." name="DC.creator" />
<meta content="White, A.H." name="DC.creator" />
<meta content="259901 Organometallic Chemistry" name="DC.subject" />
<meta content="The reactivity of meso- and rac- diastereoisomers of 2,6-bis[l-phenyl-1-(pyridin-2-yl)ethyl]pyridine {[(py)PhMeC]2C5H3N}, 2,6-bis[l,l-bis(pyridin-2-yl)ethyl]pyridine {[(py)2MeC]2C5H3N}, and the pyridin-2-ylmethanes (py)2Ph3-nCH (n = 1-3), (py)nCH4-n, (n = 2 or 3), and (py)3PhC toward
palladium(II) acetate in refluxing glacial acetic acid and at ambient temperature in organic solvents has been investigated. The nitrogen donor ligands form co-ordination derivatives in organic solvents. All except alpha-phenyl-alpha-(pyridin-2-yl)toluene [(py)Ph2CH] form identical complexes in glacial acetic acid, with (py)Ph2CH undergoing cyclometallation to form [{Pd[(py)PhHCC6H4](mu-
O2CMe)}2]. meso-[(py)PhMeC]2C5H3N, which binds as a tripodal tridentate ligand to methylmercury(II), has been shown by a single crystal X-ray study to act as a planar tridentate ligand to palladium(II) in [Pd{meso-[(pyPhMeC]2C5H3N}(O2CMe)][O2CMe].3H2O with square-planar co-ordination being completed by a unidentate acetate group. Syntheses of the new ligand [(py)2MeC]2C5H3N, with five pyridine donor groups, and alpha,alpha,alpha-tris(pyridin-2-y1)toluene [(py)3PhC] are described." name="DC.description" />
<meta content="1986" name="DC.date" />
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<h1 class="ep_tm_pagetitle">Interaction of Palladium(II) Acetate with Substituted Pyridines, including a Cyclometallation Reaction and the Structure of [Pd{meso-[(py)PhMeC]2C5H3N}(02CMe)][02CMe].3H2O</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Minchin, N.J.</span> and <span class="person_name">Skelton, B.W.</span> and <span class="person_name">White, A.H.</span> (1986) <xhtml:em>Interaction of Palladium(II) Acetate with Substituted Pyridines, including a Cyclometallation Reaction and the Structure of [Pd{meso-[(py)PhMeC]2C5H3N}(02CMe)][02CMe].3H2O.</xhtml:em> Journal of the Chemical Society, Dalton Transactions, 10 . pp. 2205-2210. ISSN 1477-9226</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/2909/1/Dalton1986_2C_2205.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" class="ep_doc_icon" border="0" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/2909/1/Dalton1986_2C_2205.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />746Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input accept-charset="utf-8" value="4263" name="docid" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://dx.doi.org/10.1039/DT9860002205">http://dx.doi.org/10.1039/DT9860002205</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The reactivity of meso- and rac- diastereoisomers of 2,6-bis[l-phenyl-1-(pyridin-2-yl)ethyl]pyridine {[(py)PhMeC]2C5H3N}, 2,6-bis[l,l-bis(pyridin-2-yl)ethyl]pyridine {[(py)2MeC]2C5H3N}, and the pyridin-2-ylmethanes (py)2Ph3-nCH (n = 1-3), (py)nCH4-n, (n = 2 or 3), and (py)3PhC toward
palladium(II) acetate in refluxing glacial acetic acid and at ambient temperature in organic solvents has been investigated. The nitrogen donor ligands form co-ordination derivatives in organic solvents. All except alpha-phenyl-alpha-(pyridin-2-yl)toluene [(py)Ph2CH] form identical complexes in glacial acetic acid, with (py)Ph2CH undergoing cyclometallation to form [{Pd[(py)PhHCC6H4](mu-
O2CMe)}2]. meso-[(py)PhMeC]2C5H3N, which binds as a tripodal tridentate ligand to methylmercury(II), has been shown by a single crystal X-ray study to act as a planar tridentate ligand to palladium(II) in [Pd{meso-[(pyPhMeC]2C5H3N}(O2CMe)][O2CMe].3H2O with square-planar co-ordination being completed by a unidentate acetate group. Syntheses of the new ligand [(py)2MeC]2C5H3N, with five pyridine donor groups, and alpha,alpha,alpha-tris(pyridin-2-y1)toluene [(py)3PhC] are described.</p></div><table style="margin-bottom: 1em" cellpadding="3" class="not_ep_block" border="0"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">2909</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">29 Jan 2008 13:51</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">29 Jan 2008 13:51</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=2909;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=2909">item control page</a></p>
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