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<title>UTas ePrints - The Magnetic Properties of the Cyclopentadienyltitanium(III) Derivatives CpTiCl2, Cp2TiCl, and Cp3Ti</title>
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<meta content="Canty, A.J." name="eprints.creators_name" />
<meta content="Coutts, R.S.P." name="eprints.creators_name" />
<meta content="Wailes, P.C." name="eprints.creators_name" />
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<meta content="The synthesis of tris(cyclopentadienyl)titanium(III) in high yield is presented. The effect on the magnetic properties of titanium trichloride of introducing successively one, two, and three cyclopentadienyl ligands is examined. CpTiC12 behaves as a magnetically dilute compound whose susceptibility follows a Curie-Weiss law, and the susceptibility (mu eff = 1.69 +/- 0.05 B.M.) indicates little if any spin-spin interaction. With two cyclopentadienyl groups present (cp2TiCl), spin-spin interaction through chlorine bridges becomes evident. The susceptibility of Cp3Ti was determined between 100 and 320 K and was found to be independent of temperature over this range. After correcting for T.I.P. and applying a Weiss constant, mu eff was found to be 1.71 B.M. The
volatility and solubility of Cp3Ti are strong indications of its monomeric nature. Infrared and electronic spectra of the solid cyclopentadienyl species and titanium trichloride were measured over the range 250-30,000 cm-1" name="eprints.abstract" />
<meta content="1968" name="eprints.date" />
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<meta content="Coutts, R.S.P." name="DC.creator" />
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<meta content="The synthesis of tris(cyclopentadienyl)titanium(III) in high yield is presented. The effect on the magnetic properties of titanium trichloride of introducing successively one, two, and three cyclopentadienyl ligands is examined. CpTiC12 behaves as a magnetically dilute compound whose susceptibility follows a Curie-Weiss law, and the susceptibility (mu eff = 1.69 +/- 0.05 B.M.) indicates little if any spin-spin interaction. With two cyclopentadienyl groups present (cp2TiCl), spin-spin interaction through chlorine bridges becomes evident. The susceptibility of Cp3Ti was determined between 100 and 320 K and was found to be independent of temperature over this range. After correcting for T.I.P. and applying a Weiss constant, mu eff was found to be 1.71 B.M. The
volatility and solubility of Cp3Ti are strong indications of its monomeric nature. Infrared and electronic spectra of the solid cyclopentadienyl species and titanium trichloride were measured over the range 250-30,000 cm-1" name="DC.description" />
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<h1 class="ep_tm_pagetitle">The Magnetic Properties of the Cyclopentadienyltitanium(III) Derivatives CpTiCl2, Cp2TiCl, and Cp3Ti</h1>
<p style="margin-bottom: 1em" class="not_ep_block"><span class="person_name">Canty, A.J.</span> and <span class="person_name">Coutts, R.S.P.</span> and <span class="person_name">Wailes, P.C.</span> (1968) <xhtml:em>The Magnetic Properties of the Cyclopentadienyltitanium(III) Derivatives CpTiCl2, Cp2TiCl, and Cp3Ti.</xhtml:em> Australian Journal of Chemistry, 21 (3). pp. 807-810. ISSN 0004-9425</p><p style="margin-bottom: 1em" class="not_ep_block"></p><table style="margin-bottom: 1em" class="not_ep_block"><tr><td valign="top" style="text-align:center"><a href="http://eprints.utas.edu.au/3008/1/AJC1968_2C_807.pdf"><img alt="[img]" src="http://eprints.utas.edu.au/style/images/fileicons/application_pdf.png" border="0" class="ep_doc_icon" /></a></td><td valign="top"><a href="http://eprints.utas.edu.au/3008/1/AJC1968_2C_807.pdf"><span class="ep_document_citation">PDF</span></a> - Full text restricted - Requires a PDF viewer<br />150Kb</td><td><form method="get" accept-charset="utf-8" action="http://eprints.utas.edu.au/cgi/request_doc"><input value="4373" name="docid" accept-charset="utf-8" type="hidden" /><div class=""><input value="Request a copy" name="_action_null" class="ep_form_action_button" onclick="return EPJS_button_pushed( '_action_null' )" type="submit" /> </div></form></td></tr></table><p style="margin-bottom: 1em" class="not_ep_block">Official URL: <a href="http://www.publish.csiro.au/nid/52/issue/3500.htm">http://www.publish.csiro.au/nid/52/issue/3500.htm</a></p><div class="not_ep_block"><h2>Abstract</h2><p style="padding-bottom: 16px; text-align: left; margin: 1em auto 0em auto">The synthesis of tris(cyclopentadienyl)titanium(III) in high yield is presented. The effect on the magnetic properties of titanium trichloride of introducing successively one, two, and three cyclopentadienyl ligands is examined. CpTiC12 behaves as a magnetically dilute compound whose susceptibility follows a Curie-Weiss law, and the susceptibility (mu eff = 1.69 +/- 0.05 B.M.) indicates little if any spin-spin interaction. With two cyclopentadienyl groups present (cp2TiCl), spin-spin interaction through chlorine bridges becomes evident. The susceptibility of Cp3Ti was determined between 100 and 320 K and was found to be independent of temperature over this range. After correcting for T.I.P. and applying a Weiss constant, mu eff was found to be 1.71 B.M. The
volatility and solubility of Cp3Ti are strong indications of its monomeric nature. Infrared and electronic spectra of the solid cyclopentadienyl species and titanium trichloride were measured over the range 250-30,000 cm-1</p></div><table style="margin-bottom: 1em" border="0" cellpadding="3" class="not_ep_block"><tr><th valign="top" class="ep_row">Item Type:</th><td valign="top" class="ep_row">Article</td></tr><tr><th valign="top" class="ep_row">Subjects:</th><td valign="top" class="ep_row"><a href="http://eprints.utas.edu.au/view/subjects/259901.html">250000 Chemical Sciences > 259900 Other Chemical Sciences > 259901 Organometallic Chemistry</a></td></tr><tr><th valign="top" class="ep_row">Collections:</th><td valign="top" class="ep_row">UNSPECIFIED</td></tr><tr><th valign="top" class="ep_row">ID Code:</th><td valign="top" class="ep_row">3008</td></tr><tr><th valign="top" class="ep_row">Deposited By:</th><td valign="top" class="ep_row"><span class="ep_name_citation"><span class="person_name">Prof Allan J Canty</span></span></td></tr><tr><th valign="top" class="ep_row">Deposited On:</th><td valign="top" class="ep_row">04 Feb 2008 15:28</td></tr><tr><th valign="top" class="ep_row">Last Modified:</th><td valign="top" class="ep_row">04 Feb 2008 15:28</td></tr><tr><th valign="top" class="ep_row">ePrint Statistics:</th><td valign="top" class="ep_row"><a target="ePrintStats" href="/es/index.php?action=show_detail_eprint;id=3008;">View statistics for this ePrint</a></td></tr></table><p align="right">Repository Staff Only: <a href="http://eprints.utas.edu.au/cgi/users/home?screen=EPrint::View&eprintid=3008">item control page</a></p>
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